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Tetrahydrofuran-d8 (THf-d8 TDf) is a deuterated NMR solvent containing 0.03% (v/v) TMS (tetramethylsilane). It is useful in NMR-based research and analyses. 1H NMR line shape analysis of the exchange rates of proton between methanol and acetic acid dissolved in THf-d8 was reported. It participates as a solvent in the synthesis of deuteriotris[bis(trimethylsilyl)amido]thorium and deuteriotris[bis(trimethylsiiyl)amido]uranium. Dynamic NMR spectroscopic study of 15N 15NAE-dipentadeuterophenylformamidine (DPfA) has been studied in THf-d8.
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